Chemistry 300                                                                                                              Fall 2004

QUANTITATIVE ANALYSIS

INSTRUCTOR: Dr. Kevin D. Crawford

                             crawfordk@citadel.edu

                                    Office: Byrd 315, Phone: 953-7787

CLASS MEETINGS: Lecture – MWF, 1:00-1:50, Lab – Wednesday, 2:00-4:50, Home base is Byrd 314.

POSTED KEYS: Homework and Exam keys will be posted outside my office.

 

OFFICE HOURS:  Monday and Wednesdays, 10-11am, Mondays 2-3pm and whenever my office door is open and I am not busy.  Appointments also welcomed.

 

ATTENDANCE:  Attendance at each class period is mandatory, and punctuality is expected.  Advance notice of unavoidable absences is required.  Make-ups will NOT be allowed for unexcused absences.  Examples of excusable absences include infirmary visits, court dates, funerals, etc.  GUARD DUTY DOES NOT EXCUSE YOU FROM A SCHEDULED EXAM.  Whenever possible, arrangements should be made in advance for absences.  Excessive unexcused absences will be dealt with at my discretion (in addition to any other punishments incurred).  The 20% rule applies - the sum of excused and unexcused absences may not exceed 20% of the class periods (9), or the student will fail the course.

 

CALCULATORS:  Each of you should have your own calculator and be able to use it.  You will not be allowed to lend or borrow calculators during a test.

 

FOOD, DRINK, TOBACCO PRODUCTS:  These items are prohibited in Byrd Hall.  Do not bring them to class and do not use them in the building.

 

TEXTBOOK:  You must have the textbook Fundamentals of Analytical Chemistry, 8th edition, by Skoog, West, Holler, and Crouch.

 

ACADEMIC HONESTY (HONOR CODE):  I expect that you will only turn in work that is of your own effort. Cheating on exams will not be tolerated.

 

GOALS AND OBJECTIVES:

            1.  To learn the fundamental principles behind the quantitative analysis of chemical compounds.

            2.  To develop an ability to conduct a quantitative analysis and report the results.

            3.  To gain experience in common methods of wet chemical analysis.

            4.  To expand a working vocabulary in both chemical terms and the english language.

            5.  To understand the limitations of quantitative analysis methods.


EXAMS:  The final exam will be semi-cumulative.  All other exams will be cumulative only as necessary to cover the current material. 

 

     NOTE:  ADHD and LD students who require special exam procedures must present documentation to me from Academic Support Services well before the first exam.

 

POINTS:  The following point breakdown will be used to determine your course grade for Chem 300:

              a.       3 exams at 100 points each                                             40%

 

              b.       Laboratory Portion                                                         40%

 

              c.       Final exam (includes Lab Practical)                                  15%

 

              d.       Worksheets and Participation                                          5%

                        -------------------------------------------------------------------------------

                        Total                                                                               100%

 


Chemistry 300                                                     Kevin D. Crawford                                 Fall 2004

      Date                           Lecture Topic                                                                                      Text Chapter

      -------                          -----------------------------------------                                                         ---------------------

      Aug 25                      Introduction, Analytical Process, Measurements                          1

      Aug 27                      Process specifics                                                                                 2

 

      Aug 30                      Process Specifics                                                                                 2

      Sep 1                          Field Trip to SC Aquarium

      Sep 3                          Spreadsheets, Stoichiometry                                                             3,4

 

      Sep 6                          Calcs Reviews, Errors                                                                          4,5

      Sep 8                          Lab Preview

      Sep 10                        Errors, Statistics                                                                                   6,7

 

      Sep 13                        Sampling, Calibrations                                                                        8

      Sep 15                        Lab (Qualifying)

      Sep 17                        Test 1

 

      Sep 20                        Equilibria                                                                                               9   

      Sep 22                        Lab (Qualifying/Solutions Prep)

      Sep 24                        Buffers                                                                                                   9

 

      Sep 27                        Activity Coefficients                                                                           10

      Sep 29                        Lab (Bottled water)                                                                                   

      Oct 1                          Complex Equilibria                                                                               11

 

      Oct 4                          Complex Equilibria                                                                               11

      Oct 6                          Lab (Bottled water)

      Oct 8                          Test 2

 

      Oct 11                        Gravimetric Analysis Applied                                                            12

      Oct 13                        Lab (Bottled water)

      Oct 15                        Titrations Applied                                                                               13

 

      Oct 18                        Titrations Applied                                                                               14

      Oct 20                        Lab (Bottled water)

      Oct 22                        Titrations Applied                                                                               15

 

      Oct 25                        Titrations Applied                                                                               16

      Oct 27                        Lab (Bottled water)

      Oct 29                        Complexation titrations                                                                       17

 

      Nov 1                         Complexation titrations                                                                       17

      Nov 3                         Lab (Bottled water)                                                                             

      Nov 5                         Test 3

 

      Nov 8                         Redox                                                                                                     18 

      Nov 10                       Lab (Bottled water)

      Nov 12                       Redox review/Electrode measurements                                            18,19

 

      Nov 15                       Electrode measurements/Redox titrations                                        19,20

      Nov 17                       Lab (Bottled water)

      Nov 19                       Redox titrations 20

 

      Nov 29                       Potentiometry                                                                                       21

      Dec 1                         Lab (final report and poster assembly)

      Dec 3                         Potentiometry/Electrogravimetry                                                      21,22

 

      Dec 6                         REVIEW/Catch-up day, Final Lab report DUE                               

      Dec 8                         FINAL EXAM – 1:00pm.